Controllable and chemo-selective conversion of sodium sulfinates to disulfides or thiosulfonates by a solvent-free mechanochemical approach



: Wang Jinjing, Liu Xiongbo, Yang Shikai, Yu Ao, Li Jinshan, Liu Hongtao, Li Jianwei, Jia Chunman

Publisher: Elsevier Ltd

: 2023

 Tetrahedron

: 133434

: 139

: 1464-5416

DOI: https://doi.org/10.1016/j.tet.2023.133434

: https://www.sciencedirect.com/science/article/pii/S0040402023002259?via%3Dihub


A solvent-free ball-milling method for synthesizing structurally diverse disulfide and thiosulfonate derivatives from readily available, odorless sodium sulfinates has been developed. This convenient mechanochemical protocol allows the rapid and chemo-selective construction of disulfides and thiosulfonates.



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