A1 Vertaisarvioitu alkuperäisartikkeli tieteellisessä lehdessä

Deposition of hydroxyapatite coatings by axial plasma spraying: Influence of feedstock characteristics on coating microstructure, phase content and mechanical properties




TekijätGanvir Ashish, Markocsan Nicolaie, Balani Kantesh, Nagar Sainyam

KustantajaELSEVIER SCI LTD

Julkaisuvuosi2021

JournalJournal of the European Ceramic Society

Tietokannassa oleva lehden nimiJOURNAL OF THE EUROPEAN CERAMIC SOCIETY

Lehden akronyymiJ EUR CERAM SOC

Vuosikerta41

Numero8

Aloitussivu4637

Lopetussivu4649

Sivujen määrä13

ISSN0955-2219

eISSN1873-619X

DOIhttps://doi.org/10.1016/j.jeurceramsoc.2021.02.050

Rinnakkaistallenteen osoitehttps://research.utu.fi/converis/portal/detail/Publication/54597703


Tiivistelmä
Axial plasma spray is one of the thermal spray techniques to deposit multifunctional advanced coatings. The present work explores the use of this process to deposit thin, continuous, and adherent Ca5 (PO4)3OH (hydroxyapatite, HAp) coatings and characterize its microstructure, phases, hardness and adhesion strength. Three different suspension-deposited HAp coatings were investigated and compared with powder-deposited HAp coating on a Ti6Al4V substrate. The effect of mean solute particle size and solid-loading in the suspension has been explored on the evolution of microstructure, phase content and mechanical properties of axial suspension plasma sprayed (ASPS) coatings. Phase-characterization has shown retention of hydroxyapatite phase and coating crystallinity in the deposited coatings, whereas the adhesion strength of the HAp coating decreased from -40 MPa to -13 MPa when bioglass was added to the feedstock material. The lower solid load content and lower mean solute particle size in the suspension were found to be beneficial in achieving porous, rougher, and welladhering coatings. This work concludes that ASPS can potentially deposit thin HAp coatings (< 50 ?m) with high adhesion strength.

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