A1 Vertaisarvioitu alkuperäisartikkeli tieteellisessä lehdessä
Synthesis of self-assembled mesoporous 3D In2O3 hierarchical micro flowers composed of nanosheets and their electrochemical properties
Tekijät: Prakasam BA, Lahtinen M, Peuronen A, Manikandan G, Muruganandham M, Sillanpaa M
Kustantaja: ROYAL SOC CHEMISTRY
Julkaisuvuosi: 2018
Journal: RSC Advances
Tietokannassa oleva lehden nimi: RSC ADVANCES
Lehden akronyymi: RSC ADV
Vuosikerta: 8
Numero: 45
Aloitussivu: 25856
Lopetussivu: 25865
Sivujen määrä: 10
ISSN: 2046-2069
DOI: https://doi.org/10.1039/c8ra03573c
Rinnakkaistallenteen osoite: https://research.utu.fi/converis/portal/Publication/36303263
This report describes the methodology for the fabrication of mesoporous In2O3 microflowers by hydrothermal and calcination procedures in which In(OH)(3)/In2S3 acts as an intermediate. Both In2O3 and its precursor were analyzed with scanning electron microscopy, energy dispersive X-ray spectrophotometry, transmission electron microscopy and powder X-ray diffraction. BET surface area, pore size and pore volume analyses were also carried out. Electron microscopy images clearly evidence the self-assembly of 2D nanosheets into the micro flower structure. The mechanism of self-assembly and calcination is reported. Electrochemical properties of the synthesized In2O3 micro flowers were studied.
Ladattava julkaisu This is an electronic reprint of the original article. |