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1-ALKYLTHIOALKYLATION OF NUCLEOSIDE HYDROXYL FUNCTIONS AND ITS SYNTHETIC APPLICATIONS - A NEW VERSATILE METHOD IN NUCLEOSIDE CHEMISTRY
Tekijät: ZAVGORODNY S, POLIANSKI M, BESIDSKY E, KRIUKOV V, SANIN A, POKROVSKAYA M, GURSKAYA G, LONNBERG H, AZHAYEV A
Kustantaja: PERGAMON-ELSEVIER SCIENCE LTD
Julkaisuvuosi: 1991
Lehti:: Tetrahedron Letters
Tietokannassa oleva lehden nimi: TETRAHEDRON LETTERS
Lehden akronyymi: TETRAHEDRON LETT
Vuosikerta: 32
Numero: 51
Aloitussivu: 7593
Lopetussivu: 7596
Sivujen määrä: 4
ISSN: 0040-4039
DOI: https://doi.org/10.1016/0040-4039(91)80543-F
Tiivistelmä
Treatment of appropriately protected nucleosides with a mixture of acetic acid, acetic anhydride and dialkylsulfoxide was shown to give O-(1-alkylthioalkylated) nucleosides that were oxidized to the corresponding sulfoxides and sulfones, or converted via O-halogenomethyl derivatives to various O-substituted nucleosides.
Treatment of appropriately protected nucleosides with a mixture of acetic acid, acetic anhydride and dialkylsulfoxide was shown to give O-(1-alkylthioalkylated) nucleosides that were oxidized to the corresponding sulfoxides and sulfones, or converted via O-halogenomethyl derivatives to various O-substituted nucleosides.
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